Eliprodil_LCMS_16508_MedChemExpress

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 19

Acq. Instrument : HY-LCMS-02 Location : P1-C-06Injection Date : 6/8/2015 11:48:49 AM Inj : 1

Inj Volume : 3.000 µl

Acq. Method : D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\100-1000MS+3MIN- 1.5_(0.02%FA).M

Last changed : 6/8/2015 10:30:13 AM by Li Shan(LCMS-02)

Analysis Method : D:\AGLIENT 1260\METHOD\HM-342_41A(RP-HPLC)N@P.M Last changed : 6/8/2015 3:39:45 PM by Li Shan(LCMS-02) (modified after loading)

Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-76,30℃

Catalog No : HY-12881 Batch#16508 A-RP-132

Additional Info : Peak(s) manually integrated

min

0.5

1

1.52

2.53mAU 0

100200300400500600 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...60\DATA\20150608\20150608 2015-06-08 10-30-13\BIZ2015-608-DJL9.D)

1.525

1.721

2.332

2.460

2.736

===================================================================== Area Percent Report =====================================================================

Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000

Do not use Multiplier & Dilution Factor with ISTDs

Signal 1: DAD1 B, Sig=214,4 Ref=off

Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %

----|-------|----|-------|----------|----------|--------| 1 1.525 MM 0.0596 11.25163 3.14747 0.3871 2 1.721 MM 0.0673 2885.34497 714.48468 99.2596 3 2.332 MM 0.0517 3.45676 1.11335 0.1189 4 2.460 MM 0.0489 3.90815 1.33153 0.1344 5 2.736 MM 0.0657 2.90489 7.37403e-1 0.0999

Totals : 2906.86641 720.81443

===================================================================== *** End of Report ***

Data File D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\BIZ2015-608-DJL9.D Sample Name: BIZ2015-608-DJL9

HY-LCMS-02 6/8/2015 3:39:47 PM Li Shan(LCMS-02)Page 1 of 1

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 19Acq. Instrument : HY-LCMS-02 Location : P1-C-06Injection Date : 6/8/2015 11:48:49 AM Inj : 1 Inj Volume : 3.000 µl Acq. Method : D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\100-1000MS+3MIN- 1.5_(0.02%FA).M Last changed : 6/8/2015 10:30:13 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\HM-342_41A(RP-HPLC)N@P.M Last changed : 6/8/2015 3:40:41 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-76,30℃ Catalog No : HY-12881 Batch#16508 A-RP-132 Additional Info : Peak(s) manually integrated min

0.51 1.52 2.530

200000

400000

600000

800000

1000000

MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\BIZ2015-608-DJL9.D) ES-API, Pos, Sca

1.731

Data File D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\BIZ2015-608-DJL9.D Sample Name: BIZ2015-608-DJL9

HY-LCMS-02 6/8/2015 3:40:43 PM Li Shan(LCMS-02)Page 1 of 2

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. Weight Time (MS) MS Area or Ion 1.731 7306397 350.10 I 349.10 I 348.10 I

m/z 1002003004005006007008009000

20

40

60

80

100

*MSD1 SPC, time=1.689:1.780 of D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\BIZ2015-608-DJL9.D ES-API,Max: 512501

330.1 351.1 349.1 348.1 *** End of Report ***

Data File D:\AGLIENT 1260\DATA\20150608\20150608 2015-06-08 10-30-13\BIZ2015-608-DJL9.D Sample Name: BIZ2015-608-DJL9

HY-LCMS-02 6/8/2015 3:40:43 PM Li Shan(LCMS-02)Page 2 of 2