CFI-400945_free_base_LCMS_23771_MedChemExpress

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

File D:\CHEM32\1\DATA\BIZ\BIZ2017-307-WJ9.D Tgt Mass (EZX): 534.20 Injection Date : 7 Mar 17 2:03 pm +0800 Seq. Line : 0 Sample Name : BIZ2017-307-WJ9 Location : P2-F-03 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No : HY-12300 Batch#23771 Easy-Access Method: '1-POS-3MIN' 534.20 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*

0.5

1

1.52

2.5mAU 0

5001000*DAD1 B, Sig=214,4 Ref=off 1.301

1.343

1.4111.422

1.508

1.613

1.724

min*

0.51

1.52

2.5mAU 0

200400

*DAD1 C, Sig=254,4 Ref=off 1.301

1.3431.4101

.4201.4781.4961.5361.6071.618

min

0.51 1.5

2

2.5

20000

4000060000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.417

min

0.5

1

1.5

2

2.5

5000

100001500020000 Ion 535.2, MSD1 535.2,Target Mass 534.2 +H Positive, EIC=534.9:535.9

1.416

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)

|-------|--------|--------------|--------------|--------|------| 1.30 0.02 2.10 1.96 0.16 ND 1.34 0.02 1284.24 1385.25 98.32 268 1.41 0.02 5.10 5.54 0.39 268 1.42 0.01 1.59 1.81 0.12 268 1.51 0.02 9.14 8.63 0.70 268 1.61 0.03 2.98 1.91 0.23 268 1.72 0.02 1.08 1.07 0.08 ND

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.30 0.02 1.54 1.03 0.23 ND 1.34 0.02 673.91 728.43 98.93 268 1.41 0.02 2.94 3.14 0.43 268 1.42 0.01 0.83 1.04 0.12 268 1.48 0.01 0.07 0.02 0.01 268 1.50 0.01 0.46 0.00 0.07 268 1.54 0.01 0.23 0.03 0.03 535

MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 3/7/2017 2:10:02 PM GZZ_718Page 1 of 3

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

MS Report from Instrument: HY-LCMS-02

1.61 0.01 0.63 0.87 0.09 535

1.62 0.01 0.63 0.74 0.09 535

HY-LCMS-02 3/7/2017 2:10:02 PM GZZ_718Page 2 of 3

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

Ret. Time: 1.42 <<<< POSITIVE SPECTRA >>>>m/z 2003004005006007008009000

2000

4000

6000

8000

10000

12000

14000

16000

ES-API Positive

536.3 535.3 268.2

MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 3/7/2017 2:10:02 PM GZZ_718Page 3 of 3